関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Alpha-Aminobutyric Acid | HCID 6657 | — |
| 反応物 | Acetic Anhydride | HCID 7918 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | 2-(Acetylamino)butanoic acid | HCID 306107 | — |
反応手順
163 g (1.58 mol) 2-aminobutanoic acid are dissolved in acetic acid, and 242 g (2.37 mol) acetic anhydride are added dropwise. The mixture is stirred for 2 h at 100° C. until completion of reaction, then the solution evaporated to dryness in vacuo. The solid residue is suspended in ethyl acetate, filtered and washed with diethyl ether.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US07087605B2 |
|---|
| 出典データセット | uspto-grants-2006_08 |
|---|
| ORD ID | ord-4825907718a34102b76de664069c39ba |
|---|
| 出典メモ | uspto-grants-2006_08 |
|---|
