関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Phenyl Isothiocyanate | HCID 7673 | — |
| 反応物 | 4,4'-Diaminobenzanilide | HCID 69917 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | 4,4'-Di(phenylthiocarbamoylamino)benzanilide | HCID 19693281 | 72.3% |
反応手順
4,4'-Diaminobenzanilide (0.658 g, 2.5 mM) was dissolved in 20 ml of acetone, and 2 equivalents of phenylisothiocyanate (0.676 g, 5 mM) was added. The mixture was stirred at 55° C. for 10 minutes. After cooling, the reaction mixture was filtered, and washed with acetone/n-hexane to obtain 0.90 g (72.3% yield) of a colorless crystal of compound A-15.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05723075 |
|---|
| 出典データセット | uspto-grants-1998_03 |
|---|
| ORD ID | ord-e8642ae0ecb248809067cd131fde0eed |
|---|
| 出典メモ | uspto-grants-1998_03 |
|---|
