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Cyclopentanecarbonyl chloride → N-[1-(3-tert-butyl-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl)propyl]cyclopentanecarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclopentanecarbonyl chloride | HCID 78284 | — |
| 反応物 | 6-(1-Aminopropyl)-3-tert-butyl-1,2,4-triazin-5(4h)-one | HCID 135594090 | — |
| 生成物 | N-[1-(3-tert-butyl-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl)propyl]cyclopentanecarboxamide | HCID 135752563 | — |
反応手順
In analogy to the procedure for Example 36A, 110 mg (0.50 mmol) 6-(1-aminopropyl)-3-tert-butyl-1,2,4-triazin-5(4H)-one, 70 mg (0.50 mmol) cyclopentanecarbonyl chloride and proportionate amounts of the other reagents are used. The crude product is used in the next step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07087605B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-b46f015255f1488ebf4026b731b6fb22 |
| 出典メモ | uspto-grants-2006_08 |