2-Chloroethanol → 2-(Pyridin-3-yloxy)ethan-1-ol

HRID 75474

反応式

HRID 75474 の反応式
[OH:1][C:2]1[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=1.Cl[CH2:9][CH2:10][OH:11].C([O-])([O-])=O.[K+].[K+]>CN(C=O)C>[N:4]1[CH:5]=[CH:6][CH:7]=[C:2]([O:1][CH2:9][CH2:10][OH:11])[CH:3]=1

参加物

5

実験手順

The yield of the title compound according to D1, starting from 3-hydroxypyridine, 2-chloroethanol and K2CO3 in DMF was 19%. The title compound has also been prepared according to EP 0 286 242 A2 starting from methyl [(3-pyridinyl)oxy]acetate.

出典と根拠

ORDレコード
ord-b440f9e1831244a0b541a4df6290b27d
出典データセット
uspto-grants-2014_09
特許番号
US08835439B2

関連ノート

読み込み中…