反応式
[NH2:1][CH:2]([C:5]1[C:6](=[O:16])[NH:7][C:8]([CH:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[N:9][N:10]=1)[CH2:3][CH3:4].[C:17](Cl)(=[O:22])[CH2:18][CH2:19][CH2:20][CH3:21]>>[CH:11]1([C:8]2[NH:7][C:6](=[O:16])[C:5]([CH:2]([NH:1][C:17](=[O:22])[CH2:18][CH2:19][CH2:20][CH3:21])[CH2:3][CH3:4])=[N:10][N:9]=2)[CH2:15][CH2:14][CH2:13][CH2:12]1参加物
3
実験手順
In analogy to the procedure for Example 36A, 150 mg (0.67 mmol) 6-(1-aminopropyl)-3-cyclopentyl-1,2,4-triazin-5(4H)-one, 90 mg (0.74 mmol) pentanoyl chloride and proportionate amounts of the other reagents are used. The crude product is used in the next step without further purification.
後処理
- customThe crude product is used in the next step without further purification
出典と根拠
- ORDレコード
- ord-526d21388cd841819a22eea236d08838
- 出典データセット
- uspto-grants-2006_08
- 特許番号
- US07087605B2
関連ノート
読み込み中…