関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Benzyl Isothiocyanate | HCID 2346 | — |
| 反応物 | 1,5-Diaminonaphthalene | HCID 16720 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | 1,5-Di(benzylthiocarbamoylamino)naphthalene | HCID 19693280 | 30.7% |
反応手順
1,5-Naphthalenediamine (0.791 g, 5 mM) was dissolved in 20 ml of ethyl acetate, and 2 equivalents of benzylisothiocyanate (1.492 g, 10 mM) were added. The mixture was stirred at 80° C. for 30 minutes. After cooling, the reaction mixture was filtered, and washed with ethylacetate/n-hexane to obtain 0.70 g (30.7% yield) of a colorless crystal of compound A-29.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05723075 |
|---|
| 出典データセット | uspto-grants-1998_03 |
|---|
| ORD ID | ord-d421bcbbd72f4cb18c2bcf8464545117 |
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| 出典メモ | uspto-grants-1998_03 |
|---|
