化工社化工社 化学情報印刷レポート · 研究参考用
1-((Tert-butoxy)carbonyl)pyrrolidine-3-carboxylic acid → HCID 178441299、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-((Tert-butoxy)carbonyl)pyrrolidine-3-carboxylic acid | HCID 2760529 | — |
| 反応物 | 2-tert-Butyl-4-butylisothiazol-5(2H)-imine | HCID 66867228 | — |
| 生成物 | HCID 178441299 | HCID 178441299 | — |
反応手順
The product from Example 92B and 1-(tert-butoxycarbonyl)pyrrolidine-3-carboxylic acid (Aldrich) were processed using the method described in Example 92C to afford the title compound. 1H NMR (DMSO-d6) δ 0.91 (t, J=7.3 Hz, 3H), 1.27-1.35 (m, 2H), 1.39 (s, 9H), 1.55-1.65 (m, 12H), 2.06-2.11 (m, 2H), 2.62-2.67 (m, 2H), 3.19-3.30 (m, 2H), 3.45-3.54 (m, 2H), 8.56 (s, 1H). MS (ESI+) m/z 410 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08835475B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-94aae191121d4af896ac3878ac76f912 |
| 出典メモ | uspto-grants-2014_09 |