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4-Amino-2-chlorophenol → 4-(2-(N-methylcarbamoyl)4-pyridyloxy)-3-chloroaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Amino-2-chlorophenol | HCID 77578 | — |
| 反応物 | 4-Chloro-N-methylpicolinamide | HCID 1476814 | — |
| 生成物 | 4-(2-(N-methylcarbamoyl)4-pyridyloxy)-3-chloroaniline | HCID 23614562 | — |
反応手順
Entry 52: According to Method A2, Step 4, 4-amino-2-chlorophenol was reacted with 4-chloro-N-methyl-2-pyridinecarboxamide, which had been synthesized according to Method A2, Step 3b, to give 4-(2-(N-methylcarbamoyl)-4-pyridyloxy)-3-chloroaniline. According to Method C1a, 4-chloro-3-(trifluoromethyl)phenyl isocyanate was reacted with 4-(2-(N-methylcarbamoyl)-4-pyridyloxy)-3-chloroaniline to afford the urea.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08841330B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-aee74da1bb3f4b4599e297c262059df5 |
| 出典メモ | uspto-grants-2014_09 |