化工社化工社 化学情報印刷レポート · 研究参考用
Dodecanoyl chloride → Dodecanoic acid, 2-(dimethylamino)-1-methylethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dodecanoyl chloride | HCID 8166 | — |
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | Dimepranol | HCID 37511 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | Dodecanoic acid, 2-(dimethylamino)-1-methylethyl ester | HCID 157516 | — |
反応手順
The (N,N-disubstituted amino)-alkanol alkanoates are readily prepared by reacting the corresponding aminoalkinol with lauroyl chloride in the presence of triethylamine. A solvent such as chloroform is optional but preferred. For example, 1-(N,N-dimethylamino)-2-propanol can be reacted with lauroyl chloride in chloroform and in the presence of triethylamine to form 1-(N,N-dimethylamino)-2-propanol dodecanoate (DAIPD).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08841345B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-bf52ec518a5245d2b9e2bd2b666bbaa9 |
| 出典メモ | uspto-grants-2014_09 |