関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Chlorocyclopentanone | HCID 12751 | — |
| 反応物 | Thiourea | HCID 2723790 | — |
| 生成物 | 3,4,5,6-Tetrahydro-2H-cyclopenta(d)(1,3)thiazol-2-imine | HCID 332255 | — |
反応手順
A mixture of 2-chlorocyclopentanone (5.0 g, 40 mmol) and thiourea (3.0 g, 40 mmol) was heated at 70° C. for 3 hours. After cooling, the solid was triturated with ethanol and collected by filtration to afford the title compound. MS (ESI) m/z 141 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08841334B2 |
|---|
| 出典データセット | uspto-grants-2014_09 |
|---|
| ORD ID | ord-d641966f5d9548f29add4af141aa5c0f |
|---|
| 出典メモ | uspto-grants-2014_09 |
|---|
