化工社化工社 化学情報印刷レポート · 研究参考用
Iodine → 5-tert-butyl-3-(tetrahydro-2H-pyran-4-yl)thiazol-2(3H)-imine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Iodine | HCID 807 | — |
| 反応物 | 3,3-Dimethylbutanal | HCID 76335 | — |
| 反応物 | 4-Aminotetrahydropyran | HCID 419223 | — |
| 反応物 | Potassium thiocyanate | HCID 516872 | — |
| 生成物 | 5-tert-butyl-3-(tetrahydro-2H-pyran-4-yl)thiazol-2(3H)-imine | HCID 68623411 | — |
反応手順
Commercially available 3,3-dimethylbutanal (Aldrich), tetrahydro-2H-pyran-4-amine (Matrix), potassium thiocyanate (Aldrich) and iodine (EMD chemicals) were processed using the method described in Example 315A to afford the title compound. MS (ESI+) m/z 241 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08841334B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-ef468d2d183b4ba09924b14ea3fde380 |
| 出典メモ | uspto-grants-2014_09 |