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Caprolactam → 6-Aminohexanoic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Caprolactam | HCID 7768 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | 6-Aminohexanoic Acid | HCID 564 | — |
反応手順
The removal of water takes place in the presence of a total of less than 20 mmol of sodium hydroxide, in aqueous solution, per kg of caprolactam. The aqueous sodium hydroxide solution for this is added to the caprolactam prior to the evaporators. The aqueous sodium hydroxide solution is to react with caprolactam to give the Na-salt of 6-aminocaproic acid. This salt, according to DD-A-202870, has the same purification effect as sodium hydroxide, but, in contrast to sodium hydroxide, does not cause any caprolactam oligomerization.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08841445B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-4141a931bb384baa9da159d84048e1fb |
| 出典メモ | uspto-grants-2014_09 |