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5-Aminopentan-1-ol → 3-(2-Chloro-4-iodo-phenylamino)-N-(5-hydroxy-pentyl)-isonicotinamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Aminopentan-1-ol | HCID 75634 | — |
| 反応物 | 3-[(2-Chloro-4-iodophenyl)amino]isonicotinic acid | HCID 57649651 | — |
| 生成物 | 3-(2-Chloro-4-iodo-phenylamino)-N-(5-hydroxy-pentyl)-isonicotinamide | HCID 11712294 | — |
反応手順
3-(2-Chloro-4-iodo-phenylamino)-N-(5-hydroxy-pentyl)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.30 mmol of 3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid (intermediate 2) and 0.40 mmol of 5-amino-pentan-1-ol. LC/MS [9.33 min; 461 (M+1)]
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08841459B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-3078f6803d9b449782468cf589995f3f |
| 出典メモ | uspto-grants-2014_09 |