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O-Methylhydroxylamine → N-Benzyloxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | O-Methylhydroxylamine | HCID 4113 | — |
| 反応物 | 3-[(2-Chloro-4-iodophenyl)amino]isonicotinic acid | HCID 57649651 | — |
| 生成物 | N-Benzyloxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide | HCID 11677348 | — |
反応手順
N-Benzyloxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.25 mmol of 3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid (intermediate 2) and 0.36 mmol of O-methyl-hydroxylamine. LC/MS [10.01 min; 480 (M+1)]
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08841459B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-b5d33fa1f90b463887abfcf524328a3e |
| 出典メモ | uspto-grants-2014_09 |