化工社化工社 化学情報印刷レポート · 研究参考用
3-Cyclopropyl-3-oxopropanenitrile → 3-Cyclopropyl-1'-methyl-1'H-[1,4']bipyrazolyl-5-ylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Cyclopropyl-3-oxopropanenitrile | HCID 9812763 | — |
| 反応物 | di-tert-butyl 1-(1-methyl-1H-pyrazol-4-yl)hydrazine-1,2-dicarboxylate | HCID 11426954 | — |
| 生成物 | 3-Cyclopropyl-1'-methyl-1'H-[1,4']bipyrazolyl-5-ylamine | HCID 70817252 | — |
反応手順
The title compound was prepared according to the method described for Preparation 296: using di-tert-butyl 1-(1-methyl-1H-pyrazol-4-yl)hydrazine-1,2-dicarboxylate (Preparation 295) and 3-cyclopropyl-3-oxopropanenitrile to afford the title compound in 48% yield, 1.7 g.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08846698B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-11eebda06cdc4a778d8bf1ce3bfc14a1 |
| 出典メモ | uspto-grants-2014_09 |