関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Trifluoroacetic acid | HCID 6422 | — |
| 反応物 | Amino-acetic acid 4-allyl-2-methoxy-phenyl ester | HCID 69920127 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Amino-acetic acid 4-allyl-2-methoxy-phenyl ester Trifluoroacetate | HCID 86674925 | — |
反応手順
To a solution of compound amino-acetic acid 4-allyl-2-methoxy-phenyl ester (0.3 g) in DCM (10 mL) was added trifluoroacetic acid (0.5 mL) drop wise at (0° C.). The mixture was allowed to stir at room temperature (25° C.) over a period of 2 h. Solvent was stripped off completely and the reaction was carried for the next step (510 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08846721B2 |
|---|
| 出典データセット | uspto-grants-2014_09 |
|---|
| ORD ID | ord-94416477fee4402b9dae8b9b83cdb00f |
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| 出典メモ | uspto-grants-2014_09 |
|---|
