関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Carbon Disulfide | HCID 6348 | — |
| 反応物 | 2,3-Diaminopyridine | HCID 9956 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | HCID 178527819 | HCID 178527819 | — |
反応手順
To a solution of pyridine-2,3-diamine (5 g) in EtOH (150 ml) was added carbon disulfide (23 mL) at room temperature. The mixture was stirred at 40° C. under Ar for 10 h. The mixture was cooled to room temperature. The resulting white solid was filtered and washed with ether to give 1H-imidazo[4,5-b]pyridine-2-thiol (5.61 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08846713B2 |
|---|
| 出典データセット | uspto-grants-2014_09 |
|---|
| ORD ID | ord-ea7d4add4185470b924efe62d498fe9b |
|---|
| 出典メモ | uspto-grants-2014_09 |
|---|
