Methyl 4-Formylbenzoate → 4-(5-Methyl-4-oxo-3-phenyl-4,5-dihydro-isoxazolo[4,3-c]pyridin-6-yl)-benzoic acid methyl ester

HRID 8311

反応式

HRID 8311 の反応式
[CH3:1][NH:2][C:3]([C:5]1[C:6]([CH3:16])=[N:7][O:8][C:9]=1[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)=[O:4].[CH3:17][O:18][C:19](=[O:28])[C:20]1[CH:25]=[CH:24][C:23]([CH:26]=O)=[CH:22][CH:21]=1>>[CH3:17][O:18][C:19](=[O:28])[C:20]1[CH:25]=[CH:24][C:23]([C:26]2[N:2]([CH3:1])[C:3](=[O:4])[C:5]3=[C:9]([C:10]4[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=4)[O:8][N:7]=[C:6]3[CH:16]=2)=[CH:22][CH:21]=1

参加物

3

反応物 2

HCID 15294Methyl 4-FormylbenzoateHCID 666631943-Methyl-5-phenyl-isoxazole-4-carboxylic acid methylamide

生成物 1

HCID 694783404-(5-Methyl-4-oxo-3-phenyl-4,5-dihydro-isoxazolo[4,3-c]pyridin-6-yl)-benzoic acid methyl ester

実験手順

This compound is obtained using 3-methyl-5-phenyl-isoxazole-4-carboxylic acid methylamide and 4-formyl-benzoic acid methyl ester in 15% as a beige solid. Mass spectrum: m/z (M+H)+: 361.2

後処理

  1. customThis compound is obtained

出典と根拠

ORDレコード
ord-b2a7a735024242189307b0a478130651
出典データセット
uspto-grants-2006_08
特許番号
US07087756B2

関連ノート

読み込み中…