Piperidine → 4-Piperidinylbut-1-ene
反応式
Br[CH2:2][CH2:3][CH:4]=[CH2:5].[NH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1>>[N:6]1([CH2:7][CH2:8][CH:9]=[CH2:10])[CH2:11][CH2:5][CH2:4][CH2:3][CH2:2]1参加物
3
実験手順
4-Bromobut-1-ene (1.35 g) was treated with piperidine (1.7 g) and heated at reflux for 3 hours. The mixture was cooled to ambient temperature, filtered and the residue washed with ether (50 mL). The combined filtrate and washings were evaporated to give the title compound (1.3 g).
後処理
- temperatureheated
- temperatureat reflux for 3 hours
- filtrationfiltered
- washthe residue washed with ether (50 mL)
- customThe combined filtrate and washings were evaporated
出典と根拠
- ORDレコード
- ord-d7ef957ab1cf46f68f1f4c42cdc7ceea
- 出典データセット
- uspto-grants-2006_08
- 特許番号
- US07087757B2
反応ノート
読み込み中…