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2,4,5-Trichloroaniline → (Methylsulfonyl)(2,4,5-trichlorophenyl)amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,4,5-Trichloroaniline | HCID 12487 | — |
| 反応物 | Methanesulfonyl chloride | HCID 31297 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | (Methylsulfonyl)(2,4,5-trichlorophenyl)amine | HCID 2427123 | — |
反応手順
A mixture of 2,4,5-trichloroaniline (39.3 g.), methane sulfonyl chloride (22.9 g.) and 100 ml. of xylene were heated together under reflux conditions for 18 hours. The mixture was then allowed to cool, which formed a brown precipitate. The product was worked up in the same manner as set forth in Example 1 to yield 24.0 g. of product, m.p. 144°-145° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04093445 |
| 出典データセット | uspto-grants-1978_06 |
| ORD ID | ord-821e4309e95646ffa6a425d6d741ea1e |
| 出典メモ | uspto-grants-1978_06 |