化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → 1-(1-Chloroethyl)-3-methoxybenzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | (+-)-1-(3-Methoxyphenyl)ethanol | HCID 90902 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 1-(1-Chloroethyl)-3-methoxybenzene | HCID 12861413 | — |
反応手順
Into a solution of 152.1 g (1 mol) of 1-(3'-methoxyphenyl)-ethan-1-ol in 750 ml petroleum ether, one introduces hydrogen chloride during ice cooling until water separation is completed. The organic phase is then washed with ice-cold water, dried and the petroleum ether is removed in vacuo. The thermo-labile residue is used without any further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04094994 |
| 出典データセット | uspto-grants-1978_06 |
| ORD ID | ord-741b9bf5f4a34758aa2a5e85ba27fdb7 |
| 出典メモ | uspto-grants-1978_06 |