alpha-Methylene-gamma-Butyrolactone Acrylic Acid → alpha-Methylene-gamma-Valerolactone Acrylic Acid
反応式
[CH2:1]=[C:2]1[CH2:7][CH2:6][O:5][C:3]1=[O:4].[C:8]([OH:12])(=[O:11])[CH:9]=[CH2:10]>CS(C)=O>[CH2:1]=[C:2]1[CH2:7][CH:6]([CH3:8])[O:5][C:3]1=[O:4].[C:8]([OH:12])(=[O:11])[CH:9]=[CH2:10]参加物
3
実験手順
To a scintillation vial was added 267 mg of the poly(α-methylene-γ-butyrolactone-acrylic acid) prepared in Example 14 and 5.14 mL DMSO on a platform shaker. Once dissolved, the solution was pipetted onto a foil-lined steel panel and placed in a 100° C. oven. Vacuum was applied to remove the solvent over approximately 60 minutes. The result was a 2 cm×2 cm transparent poly(α-methylene-γ-valerolactone-acrylic acid) film.
後処理
- dissolutionOnce dissolved
- customplaced in a 100° C.
- customto remove the solvent over approximately 60 minutes
出典と根拠
- ORDレコード
- ord-ffd324aa38484223a081589824c36559
- 出典データセット
- uspto-grants-2014_09
- 特許番号
- US08846817B2
反応ノート
読み込み中…