化工社化工社 化学情報印刷レポート · 研究参考用
Butyl Acrylate → alpha-Methylene-gamma-butyrolactone n-butyl acrylate acrylic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Butyl Acrylate | HCID 8846 | — |
| 反応物 | alpha-Methylene butyrolactone | HCID 68352 | — |
| 生成物 | alpha-Methylene-gamma-butyrolactone n-butyl acrylate acrylic acid | HCID 86762800 | — |
反応手順
Similar to Example 51, with the following exception: 3.390 g (3.46×10−2 mol) α-methylene-γ-butyrolactone and 1.075 g (8.39×10−3 mol) n-butyl acrylate were used in the monomer mixture, yielding a polymer with a glass transition temperature of 145° C. Comparison to the Fox equation suggests the statistical copolymer contains approximately 11% n-butyl acrylate repeat units.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08846817B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-01b081e27a914390b17b8bb8f541974c |
| 出典メモ | uspto-grants-2014_09 |