関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Benzene | HCID 241 | — |
| 反応物 | 1,2-Diethenylbenzene | HCID 66666 | — |
| 反応物 | gamma-Methyl-alpha-methylene-gamma-butyrolactone | HCID 99939 | — |
| 生成物 | alpha-Methylene-gamma-Valerolactone Divinyl Benzene | HCID 86664985 | — |
反応手順
To a dry 100 mL round bottom flask equipped with a magnetic stir bar was charged 1.0153 g (8.98×10−3 mol) α-methylene-γ-valerolactone, 16.78 g (0.215 mol) benzene, 0.0561 g (4.31×10−4 mol) divinyl benzene, and 0.0067 g (4.08×10−5 mol) azobisisobutylnitrile. The reactor was purged with nitrogen for 30 minutes before heating to 65° C. The reactor was held at 65° C. for 5 hours before letting cooling the reaction mixture to room temperature and drying under vacuum.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US08846817B2 |
|---|
| 出典データセット | uspto-grants-2014_09 |
|---|
| ORD ID | ord-cc45147e8cd34e0daca082f656717305 |
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| 出典メモ | uspto-grants-2014_09 |
|---|
