Isobutyric anhydride → HCID 20322014、化合物
反応式
CC1C=C2C=CC=CN2N=1.C(OC(=O)C(C)C)(=O)C(C)C.[C:22]([C:27]1[C:28]([CH3:36])=[N:29][N:30]2[CH:35]=[CH:34][CH:33]=[CH:32][C:31]=12)(=O)[CH:23]([CH3:25])[CH3:24]>S(=O)(=O)(O)O>[CH2:22]([C:27]1[C:28]([CH3:36])=[N:29][N:30]2[CH:35]=[CH:34][CH:33]=[CH:32][C:31]=12)[CH:23]([CH3:25])[CH3:24]参加物
5
実験手順
2-Methylpyrazolo[1,5-a]pyridine was worked up according to the same process as shown in example 1, with an excess isobutyric anhydride in the presence of 2-3 drops of concentrated sulfuric acid to prepare 3-isobutyryl-2-methylpyrazolo[1,5-a]pyridine (139-140°/5 mmHg). Yield 40%.
出典と根拠
- ORDレコード
- ord-63f70b4ee1244ea0ace67cf5731b45cc
- 出典データセット
- uspto-grants-1978_06
- 特許番号
- US04097483
反応ノート
読み込み中…