化工社化工社 化学情報印刷レポート · 研究参考用
Desipramine Hydrochloride → Desipramine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Desipramine Hydrochloride | HCID 65327 | — |
| 溶媒 | Sodium Hydroxide | HCID 14798 | — |
| 生成物 | Desipramine | HCID 2995 | 99.1% |
反応手順
To 6.02 g of desipramine hydrochloride was added 150 ml of 1N NaOH. The mixture was allowed to stir for 10 minutes. The aqueous mixture was extracted with 6×100 ml of chloroform. The combined chloroform layer was washed with 200 ml of water. The organic part was dried (Na2SO4) and concentrated to give 5.25 g of desipramine free base.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06368814B1 |
| 出典データセット | uspto-grants-2002_04 |
| ORD ID | ord-78cbff80e04c44a7a384b30c58aff007 |
| 出典メモ | uspto-grants-2002_04 |