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HRID 842331作成日:2026年10月27日

Sodium Hydroxide → 1,3-Dihydroisobenzofuran

https://huagongshe.com/reaction/842331

反応式

関与物質

役割名称HCID仕込み量
反応物Sodium HydroxideHCID 14798—
反応物1,2-BenzenedimethanolHCID 69153—
生成物1,3-DihydroisobenzofuranHCID 1032796%

反応手順

The procedure of Example 15 was performed except that the pH of the reaction mixture was regulated to 12 by use of sodium hydroxide. The reaction mixture was sampled for analysis. Formation of α,α′-dihydroxy-o-xylene was not observed. Instead, phthalan was formed at a yield of 96% based on α,α′-dichloro-o-xylene.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06372921B1
出典データセットuspto-grants-2002_04
ORD IDord-691be264de8b49cb99250fc961fc3048
出典メモuspto-grants-2002_04