化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → 1,3-Dihydroisobenzofuran
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 1,2-Benzenedimethanol | HCID 69153 | — |
| 生成物 | 1,3-Dihydroisobenzofuran | HCID 10327 | 96% |
反応手順
The procedure of Example 15 was performed except that the pH of the reaction mixture was regulated to 12 by use of sodium hydroxide. The reaction mixture was sampled for analysis. Formation of α,α′-dihydroxy-o-xylene was not observed. Instead, phthalan was formed at a yield of 96% based on α,α′-dichloro-o-xylene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06372921B1 |
| 出典データセット | uspto-grants-2002_04 |
| ORD ID | ord-691be264de8b49cb99250fc961fc3048 |
| 出典メモ | uspto-grants-2002_04 |