化工社化工社 化学情報印刷レポート · 研究参考用
Water → Astaxanthin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Sodium Iodide | HCID 5238 | — |
| 反応物 | Sodium Chlorate | HCID 516902 | — |
| 反応物 | Zeaxanthin | HCID 5280899 | — |
| 溶媒 | Chloroform | HCID 6212 | — |
| 生成物 | Astaxanthin | HCID 5281224 | — |
反応手順
Zeaxanthin (50 mg) was stirred in 20 ml of chloroform under nitrogen. To this stirred mixture, 200 mg of sodium chlorate and 50 mg of sodium iodide in 10 ml of water was added. The mixture was acidified slowly with 1 ml of 27% sulfuric acid. The reaction was stirred at room temperature. After 5 hours, a significant quantity of astaxanthin had formed. The reaction was worked up by addition of 1 ml of 40% sodium hydroxide, separation of the organic solution and evaporation to yield astaxanthin.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06376717B2 |
| 出典データセット | uspto-grants-2002_04 |
| ORD ID | ord-5a002155ec6d4801ac300abd4f20e80b |
| 出典メモ | uspto-grants-2002_04 |