Benzenamine, 2-chloro-N-methyl- → N-(2-chlorophenyl)-N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide

HRID 84460

反応式

HRID 84460 の反応式
[S:1]1[C:5]2[C:6]3[CH:14]=[CH:13][CH:12]=[CH:11][C:7]=3[O:8][CH2:9][CH2:10][C:4]=2[CH:3]=[C:2]1[C:15]([OH:17])=O.[Cl:18][C:19]1[CH:26]=[CH:25][CH:24]=[CH:23][C:20]=1[NH:21][CH3:22]>>[Cl:18][C:19]1[CH:26]=[CH:25][CH:24]=[CH:23][C:20]=1[N:21]([CH3:22])[C:15]([C:2]1[S:1][C:5]2[C:6]3[CH:14]=[CH:13][CH:12]=[CH:11][C:7]=3[O:8][CH2:9][CH2:10][C:4]=2[CH:3]=1)=[O:17]

参加物

3

反応物 2

HCID 136736Benzenamine, 2-chloro-N-methyl-HCID 568340534,5-Dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxylic acid

生成物 1

HCID 56680186N-(2-chlorophenyl)-N-methyl-4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxamide

実験手順

Following General Procedure C, 157 is prepared from 4,5-dihydrobenzo[b]thieno[2,3-d]oxepine-2-carboxylic acid and 2-chloro-N-methylaniline. MS: (ESI+) 70.1

出典と根拠

ORDレコード
ord-0a69fed7c2f34de79179d8e5b3b6401f
出典データセット
uspto-grants-2014_09
特許番号
US08846762B2

関連ノート

読み込み中…