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HRID 844853作成日：2026年10月26日

2-(2-Methylethyl)-6-methylbenzoic acid → N-[[2-(2-methylethyl)-6-methylphenyl]carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine

https://huagongshe.com/reaction/844853

反応式

関与物質

役割名称HCID仕込み量
反応物2-(2-Methylethyl)-6-methylbenzoic acidHCID 22613748—
反応物4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl esterHCID 69336975—
生成物N-[[2-(2-methylethyl)-6-methylphenyl]carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanineHCID 69336578—

反応手順

N-[[2-(2-methylethyl)-6-methylphenyl]carbonyl]-4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine was prepared from 4-(1,3,6-trimethyl-2,4-dioxo-5-pyrimidinyl)-L-phenylalanine methyl ester and 2-(2-methylethyl)-6-methylbenzoic acid using the general procedures described in example 7 and was obtained as an amorphous white solid. ES-HRMS m/e calcd for C27H31N3O5 (M+Na) 500.2156, found 500.2160.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06380387B1
出典データセットuspto-grants-2002_04
ORD IDord-c92b869201b54800aba333425698294b
出典メモuspto-grants-2002_04