化工社化工社 化学情報印刷レポート · 研究参考用
Saccharin → Glycidyl methacrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Saccharin | HCID 5143 | — |
| 反応物 | Dimethyl-p-toluidine | HCID 7471 | — |
| 反応物 | Dicyandiamide | HCID 10005 | — |
| 反応物 | Chlortoluron | HCID 27375 | — |
| 反応物 | Tert-butyl cumene peroxide | HCID 76997 | — |
| 反応物 | Phosphorohydrazidic acid, diethyl ester | HCID 143340 | — |
| 生成物 | Glycidyl methacrylate | HCID 7837 | — |
反応手順
Mixure A (20.0 g) is mixed with dicyandiamide (0.4 g) and N-(3-chloro-4-methylphenyl)-N',N'-dimethylurea (0.4 g) and the mixture milled in a triple-roll mill until homogeneous. The milled product is then treated with tert.butyl cumyl peroxide (0.5 g), N,N-dimethyl-p-toluidine (0.1 g), o-benzoic sulphimide (0.1 g) and diethyl phosphoro hydrazidate (0.2 g) and mixed until homogeneous.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04755571 |
| 出典データセット | uspto-grants-1988_07 |
| ORD ID | ord-0e683cd1b9c24f10a8ff55d7aabcd417 |
| 出典メモ | uspto-grants-1988_07 |