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HRID 846561作成日:2026年10月27日

(1,1'-Biphenyl)-4-carbonitrile, 4'-(nonyloxy)- → 4'-(Nonyloxy)[1,1'-biphenyl]-4-carboxylic acid

https://huagongshe.com/reaction/846561

反応式

関与物質

役割名称HCID仕込み量
反応物(1,1'-Biphenyl)-4-carbonitrile, 4'-(nonyloxy)-HCID 100887—
反応物4'-(Octyloxy)-[1,1'-biphenyl]-4-carboxylic acidHCID 2802556—
生成物4'-(Nonyloxy)[1,1'-biphenyl]-4-carboxylic acidHCID 3620263—

反応手順

In the synthesis of 4'-octyloxybiphenyl-4-caboxylic acid of Example 12, the same hydrolysis as in Example 12 was repeated except that 4'-nonyloxy-4-cyanobiphenyl was used instead of 4'-octyloxy-4-cyanobiphenyl to obtain 4'-nonyloxybiphenyl-4-carboxylic acid. This 4'-nonyloxybiphenyl-4-carboxylic acid was condensed with 4-(2-methylnonanoyl) phenol in the same manner as in the synthesis of 4-(2-methylnonanoyl) phenyl, 4'-octyloxybiphenyl-4-carboxylic acid ester of Example 13 to synthesize 4-(2-methylnonanoyl)phenyl, 4'-nonyloxybiphenyl-4-carboxylic acid ester having the aforementioned physical and chemical properties.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05137653
出典データセットuspto-grants-1992_08
ORD IDord-f7f9dc8d344f4e3797a454eaafb375b7
出典メモuspto-grants-1992_08