1-Hexadecylthio-3-trityloxy-2-propanol → 1-Hexadecylthio-3-(3-iodopropylsulfonylamino)-2-methylcarbamoyloxypropane
反応式
ClCCCCS(NCC(OC)C[O:13][C:14](=O)[NH:15][CH2:16]CCCCCCCCCCCCCCCCC)(=O)=O.[CH2:37]([S:53][CH2:54][CH:55]([OH:77])[CH2:56]OC(C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1)[CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH3:52].C(SCC(OC)C[NH:98][S:99]([CH2:102][CH2:103][CH2:104][I:105])(=[O:101])=[O:100])CCCCCCCCCCCCCCC>>[CH2:37]([S:53][CH2:54][CH:55]([O:77][C:14](=[O:13])[NH:15][CH3:16])[CH2:56][NH:98][S:99]([CH2:102][CH2:103][CH2:104][I:105])(=[O:100])=[O:101])[CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH2:45][CH2:46][CH2:47][CH2:48][CH2:49][CH2:50][CH2:51][CH3:52]参加物
4
反応物 3
生成物 1
実験手順
3-(3-Chloropropylsulfonylamino)-1-hexadecylthio-2-methylcarbamoyloxypropan III c1 is allowed to react and worked up by the same procedure as described in (5). The summary of the experimental condition and the physical data of the product are listed in the Table 8.