Phthalimide → 2-Methoxycarbonylamino-3-octadecylcarbamoyloxypropylamine

HRID 846983ノート

反応式

HRID 846983 の反応式
CO[NH:3][C:4]([CH:6]([CH2:9][O:10][C:11](=[O:31])[NH:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])CO)=O.C(SC[CH:50]([O:53]C)CN)CCCCCCCCCCCCCCC.[C:55]1(=[O:65])[NH:59]C(=O)C2=CC=CC=C12>>[CH3:50][O:53][C:55]([NH:59][CH:6]([CH2:9][O:10][C:11](=[O:31])[NH:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30])[CH2:4][NH2:3])=[O:65]

参加物

4

反応物 3

HCID 6809PhthalimideHCID 149922653-Hexadecylthio-2-methoxypropylamineHCID 198842322-Methoxycarbamoyl-3-octadecylcarbamoyloxypropanol

生成物 1

HCID 148350002-Methoxycarbonylamino-3-octadecylcarbamoyloxypropylamine

実験手順

2-Methoxycarbamoyl-3-octadecylcarbamoyloxypropanol V e1 is allowed to react and worked up by the same procedure as described in (3). The phthalimide derivative: m.p. 128°-129° C., the amine derivative: 85°-86° C. The summary of the experimental condition and the physical data of the product are listed in Tables 5 and 6.

後処理

  1. customto react
  2. custom85°-86° C

出典と根拠

ORDレコード
ord-17d0dd45925943cf9e8ce43a1a304d9b
出典データセット
uspto-grants-1992_08
特許番号
US05138067

反応ノート

読み込み中…