1-Butanol → Butoxy(triethyl)silane

HRID 847488ノート

反応式

HRID 847488 の反応式
[CH2:1]([OH:5])[CH2:2][CH2:3][CH3:4].[CH2:6]([Si:8]([CH2:12][CH3:13])([CH2:10][CH3:11])Cl)[CH3:7].Cl>[Cl-].C([N+](CC)(CC)CC1C=CC=CC=1)C.CC1C=CC(C)=CC=1>[CH2:1]([O:5][Si:8]([CH2:12][CH3:13])([CH2:10][CH3:11])[CH2:6][CH3:7])[CH2:2][CH2:3][CH3:4]

参加物

6

反応物 3

HCID 2631-ButanolHCID 313Hydrochloric AcidHCID 13819Chlorotriethylsilane

生成物 1

HCID 525735Butoxy(triethyl)silane

試薬・触媒・溶媒 2

HCID 66133Benzyl triethylammonium chloride触媒HCID 7809P-Xylene溶媒

実験手順

0.1 moles of n-butanol, 0.15 moles of triethylchlorosilane and 0.0005 moles of triethylbenzyl ammonium chloride in 50 ml of p-xylene were heated under reflux (80°-110° C.). When the evolution of HCl had ceased, the product was worked up by fractional distillation at reduced pressure.

後処理

  1. temperatureunder reflux (80°-110° C.)
  2. distillationthe product was worked up by fractional distillation at reduced pressure

出典と根拠

ORDレコード
ord-adda96e4f7b048839a4c5ba7b0701f31
出典データセット
uspto-grants-1992_08
特許番号
US05142081

反応ノート

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