Toluene → Pentaerythritol diphosphite
反応式
[OH:1][P:2]([O:4][P:5]([OH:7])[OH:6])[OH:3].Cl[C:9](Cl)([C:11]([CH2:16][OH:17])([CH2:14][OH:15])[CH2:12][OH:13])[OH:10].C1(C)C=CC=CC=1>C(N(CC)CC)C>[OH:1][P:2]([O:4][P:5]([OH:7])[OH:6])[OH:3].[OH:10][CH2:9][C:11]([CH2:16][OH:17])([CH2:14][OH:15])[CH2:12][OH:13]参加物
4
実験手順
Dichloro pentaerythritol diphosphite (1 mol) was reacted with 2.05 mol of ABITOL in toluene using 2.1 mol of triethyl amine as an acid acceptor. The very viscous liquid product, bis abietyl pentaerythritol diphosphite, was obtained after filtering the triethylamine hydrochloride and stripping the toluene.
出典と根拠
- ORDレコード
- ord-009fbb8e226d4c5f81aee465c625fa5c
- 出典データセット
- uspto-grants-1992_08
- 特許番号
- US05142083
反応ノート
読み込み中…