化工社化工社 化学情報印刷レポート · 研究参考用
Ethylene → n-Dodecylethyldichlorosilane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylene | HCID 6325 | — |
| 反応物 | n-Dodecyldichlorosilane | HCID 123720552 | — |
| 溶媒 | Isopropanol | HCID 3776 | — |
| 生成物 | n-Dodecylethyldichlorosilane | HCID 20564956 | — |
反応手順
Resultant n-dodecyldichlorosilane in an amount of 161.4 g (0.6 mol), 22.4 g of ethylene (0.8 mol) and a solution of H2PtCl6 ·6H2O in isopropanol (0.05 mol % relative to n-dodecyldichlorosilane) were charged in a pressure-proof stainless steel reactor. After sealing, reaction was carried out at 50° C. for 25 hours to give n-dodecylethyldichlorosilane [(n--C12H25)(C2H5)SiCl2 ].
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04297499 |
| 出典データセット | uspto-grants-1981_10 |
| ORD ID | ord-3fda26a631f947ffb97d341e6f053fd4 |
| 出典メモ | uspto-grants-1981_10 |