化工社化工社 化学情報印刷レポート · 研究参考用
1-Octadecene → Octadecyldichlorosilane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Octadecene | HCID 8217 | — |
| 反応物 | Dichlorosilane | HCID 61330 | — |
| 生成物 | Octadecyldichlorosilane | HCID 102243275 | — |
反応手順
Dichlorosilane in an amount of 60.6 g (0.6 mol), 176.4 g of 1-octadecene (0.7 mol) and 0.07 mol % of RhCl(PPh)3 (relative to dichlorosilane) were charged in a 500 ml pressure-proof stainless steel reactor. After sealing, reaction was carried out at 130° C. for 30 hours. The reacted liquid was distilled in vacuo to give n-octadecyldichlorosilane (n--C18H37SiHCl2).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04297499 |
| 出典データセット | uspto-grants-1981_10 |
| ORD ID | ord-752d3d99fdca4c918514c3964109bad8 |
| 出典メモ | uspto-grants-1981_10 |