化工社化工社 化学情報印刷レポート · 研究参考用
Hydrochloric Acid → HCID 178479039、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 6-Benzylpyridin-2-amine | HCID 93902 | — |
| 触媒 | Platinum oxide (PtO) | HCID 82844 | — |
| 生成物 | HCID 178479039 | HCID 178479039 | — |
反応手順
The 2-amino-6-benzylpyridine was reduced as in Example 94, except platinum oxide was used as the catalyst. The product was obtained as an oil which was dissolved in 1 N HCl and lyophilized to give a white solid. The solid was recrystallized from EtOAc to give the desired title compound as white crystals. The analysis of the product was found to be consistent with the proposed structure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06011028 |
| 出典データセット | uspto-grants-2000_01 |
| ORD ID | ord-ab961bebbe72482badb3276f57ec740a |
| 出典メモ | uspto-grants-2000_01 |