化工社化工社 化学情報印刷レポート · 研究参考用
Benzaldehyde → 1-Nitro-2-phenylethane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzaldehyde | HCID 240 | — |
| 反応物 | O-Phenylenediamine | HCID 7243 | — |
| 反応物 | beta-nitrostyrene, (E)- | HCID 5284459 | — |
| 生成物 | 1-Nitro-2-phenylethane | HCID 80208 | 95% |
反応手順
Example 219 A) trans-b-Nitrostyrene (63.0 g, 0.42 mole) was reacted with benzaldehyde (53.4 g, 0.5 mole) and 1,2-diaminobenzene (54.4 g, 0.5 mole) according to the procedure of Chikashita et. al. (Synth. Commun. 1985, 15 (6), 527) to yield (2-nitroethyl)benzene (60.0 g, 95%) as a yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06011028 |
| 出典データセット | uspto-grants-2000_01 |
| ORD ID | ord-fa6a597758a845449a7c3c11fe37506c |
| 出典メモ | uspto-grants-2000_01 |