関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Chloride | HCID 312 | — |
| 反応物 | Ethylenediaminetetraacetic Acid | HCID 6049 | — |
| 反応物 | Acrylamide | HCID 6579 | — |
| 反応物 | Ethyl Acrylate | HCID 8821 | — |
| 反応物 | 2,2'-Azobis[2-(2-imidazolin-2-yl)propane] dihydrochloride | HCID 9949101 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Acrylamide | HCID 6579 | — |
| 生成物 | MeCl EA | HCID 23497919 | — |
反応手順
A 10% solution of poly(AMD/DMAEA.MeCl/EA) was prepared as follows: 13.87 parts of 53.58% aqueous acrylamide (AMD), 25.31 parts of a 80% aqueous solution of ethacryloxyethyltrimethylammonium chloride (DMAEA.NeCI), 2.33 parts of ethyl acrylate (EA), 0.3 part EDTA, 258.16 parts of deionized water and 0.030 parts of VA-044 were added to a suitable glass vessel. The solution was sparged with nitrogen gas and stirred for about one hour at ambient temperature. The nitrogen sparge was changed to a nitrogen purge, and polymerization was initiated thermally by raising the temperature of the solution to 44° C. Stirring and heating were continued for about 21 hours to give a clear, viscous solution of poly(AMD/DMAEA.MeCl/EA) having a standard viscosity of about 2.0 centipoise.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06013708 |
|---|
| 出典データセット | uspto-grants-2000_01 |
|---|
| ORD ID | ord-d6ebacdaf4fe400d95459d14b01afbbe |
|---|
| 出典メモ | uspto-grants-2000_01 |
|---|
