Hydrochloric Acid → HCID 67167889、化合物
反応式
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4](/[CH:8]=[CH:9]/[N+:10]([O-:12])=[O:11])[C:3]=1[O:13]COC.Cl>CO.O1CCOCC1>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[C:4](/[CH:8]=[CH:9]/[N+:10]([O-:12])=[O:11])[C:3]=1[OH:13]参加物
5
実験手順
To a suspension of Example 383B in methanol (15 mL) was added 4 N HCl in dioxane (1 mL). The mixture was stirred for 4 hours, concentrated, and diluted with water. The precipitates were collected to afford the titled compound.
後処理
- concentrationconcentrated
- additiondiluted with water
- customThe precipitates were collected
出典と根拠
- ORDレコード
- ord-eda001caede046d5b5e12f4a20bc9b01
- 出典データセット
- uspto-grants-2014_09
- 特許番号
- US08846951B2
反応ノート
読み込み中…