Methyl chloromethoxyacetate → Methyl 1,2,3-triazol-1-ylmethoxyacetate

反応式

[NH:1]1[CH:5]=[CH:4][N:3]=[N:2]1.Cl[CH2:7][O:8][CH2:9][C:10]([O:12][CH3:13])=[O:11]>>[N:1]1([CH2:7][O:8][CH2:9][C:10]([O:12][CH3:13])=[O:11])[CH:5]=[CH:4][N:3]=[N:2]1

参加物

反応物 2

HCID 22034352Methyl chloromethoxyacetate

HCID 178418936HCID 178418936、化合物

生成物 1

HCID 19365964Methyl 1,2,3-triazol-1-ylmethoxyacetate

実験手順

The title compound was prepared from 1,2,3-triazole and methyl chloromethoxyacetate by a similar method to that of Preparation 40 as a colourless oil which was characterised by NMR. 1H-NMR (300 MHz, CDCl3): δ=3.76 (s,3H), 4.16 (s,2H), 5.84 (s,2H), 7.80 (d,2H) ppm.

出典と根拠

ORDレコード: ord-1831e4d6f38c42d1ac486fd9e311b0b8
出典データセット: uspto-grants-2000_01
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06015825

反応ノート

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