化工社化工社 化学情報印刷レポート · 研究参考用
Acetic acid, bromo-, propyl ester → 10-bromo-2-n-propoxycarbonylmethyloxy-5-(3-pyridylmethyl)-4H-pyrido [3,2,1-jk]carbazole-4-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic acid, bromo-, propyl ester | HCID 141981 | — |
| 反応物 | 10-bromo-2-hydroxy-5-(3-pyridylmethyl)-4H-pyrido[3,2,1-jk]carbazole-4-one | HCID 15886910 | — |
| 生成物 | 10-bromo-2-n-propoxycarbonylmethyloxy-5-(3-pyridylmethyl)-4H-pyrido [3,2,1-jk]carbazole-4-one | HCID 15886914 | 55% |
反応手順
The procedure of Example 3 was repeated by using 10-bromo-2-hydroxy-5-(3-pyridylmethyl)-4H-pyrido[3,2,1-jk]carbazole-4-one (250 mg) and n-propyl bromoacetate (0.1 ml) to obtain the title compound (170 mg, 55%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06018046 |
| 出典データセット | uspto-grants-2000_01 |
| ORD ID | ord-f19c4576aba94882bcb6692696660357 |
| 出典メモ | uspto-grants-2000_01 |