1,1,1,3,3,3-Hexachloropropane → Vinylidene chloride

HRID 850850

反応式

HRID 850850 の反応式
[F:1][C:2]([F:8])([F:7])[CH2:3][CH:4]([F:6])[F:5].[Cl:9][C:10](Cl)([Cl:16])[CH2:11]C(Cl)(Cl)Cl>C(Cl)(Cl)(Cl)Cl>[C:10]([Cl:16])([Cl:9])=[CH2:11].[F:1][C:2]([F:8])([F:7])[CH2:3][C:4]([F:6])([F:5])[Cl:9]

参加物

5

反応物 2

HCID 192151,1,1,3,3,3-HexachloropropaneHCID 680301,1,1,3,3-Pentafluoropropane

生成物 2

HCID 6366Vinylidene chlorideHCID 680311-Chloro-1,1,3,3,3-pentafluoropropane

試薬・触媒・溶媒 1

HCID 5943Carbon Tetrachloride溶媒

実験手順

The known methods of producing 1,1,1,3,3-pentafluoropropane are as follows. Carbon tetrachloride and vinylidene chloride are prepared and an addition reaction is triggered. The reaction product, 1,1,1,3,3,3-hexachloropropane, is fluorinated to produce 1,1,1,3,3-pentafluoro-3-chloropropane which is reduced with hydrogen to produce 1,1,1,3,3-pentafluoropropane (WO 95/04022).

後処理

  1. additionan addition reaction

出典と根拠

ORDレコード
ord-94614a3a7a2b489cba3e353a325d29de
出典データセット
uspto-grants-2000_01
特許番号
US06018084

関連ノート

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