化工社化工社 化学情報印刷レポート · 研究参考用
2-Methylbenzimidazole → 1-[2-(2-Methoxyethoxy)ethyl]-2-methyl-1H-benzimidazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methylbenzimidazole | HCID 11984 | — |
| 反応物 | Ethane, 1-(2-chloroethoxy)-2-methoxy- | HCID 94934 | — |
| 生成物 | 1-[2-(2-Methoxyethoxy)ethyl]-2-methyl-1H-benzimidazole | HCID 4474278 | 78% |
反応手順
1-[2-(2-Methoxyethoxy)ethyl]-2-methyl-1H-benzimidazole was synthesized as in Synthesis Example 1 except that an equimolar amount of 2-methylbenzimidazole was used instead of benzimidazole and an equimolar amount of 2-chloroethyl 2-methoxyethyl ether was used instead of 2-chloroethyl methyl ether. Yield 78%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07252925B2 |
| 出典データセット | uspto-grants-2007_08 |
| ORD ID | ord-039741a18ff34bcf95544b62301747df |
| 出典メモ | uspto-grants-2007_08 |