化工社化工社 化学情報印刷レポート · 研究参考用
(4-Acetylsulfanyl-2-methyl-phenoxy)-acetic acid tert-butyl ester → {2-Methyl-4-[5-(4-trifluoromethoxy-phenyl)-pent-4-ynylsulfanyl]-phenoxy}-acetic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (4-Acetylsulfanyl-2-methyl-phenoxy)-acetic acid tert-butyl ester | HCID 11572955 | — |
| 反応物 | Methanesulfonic acid 5-(4-trifluoromethoxy-phenyl)-pent-4-ynyl ester | HCID 11616756 | — |
| 生成物 | {2-Methyl-4-[5-(4-trifluoromethoxy-phenyl)-pent-4-ynylsulfanyl]-phenoxy}-acetic acid tert-butyl ester | HCID 11518617 | — |
反応手順
In analogy to the procedure described in example 1D], (4-acetylsulfanyl-2-methyl-phenoxy)-acetic acid tert-butyl ester (example 4A]) was reacted with methanesulfonic acid 5-(4-trifluoromethoxy-phenyl)-pent-4-ynyl ester (example 1G]) to give the title compound a light yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07253192B2 |
| 出典データセット | uspto-grants-2007_08 |
| ORD ID | ord-0aee6a9c83e7475b897de2df4e99aeb0 |
| 出典メモ | uspto-grants-2007_08 |