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Butylamine → Phenyl n-butylcarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Butylamine | HCID 8007 | — |
| 反応物 | Hexane | HCID 8058 | — |
| 反応物 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | Phenyl n-butylcarbamate | HCID 97513 | 71.97% |
反応手順
n-Butylamine (4.9 ml, 50 mmol) was used for the same reaction as in Production Example 310-1, and purification was performed by silica gel column chromatography (hexane:ethyl acetate=4:1) to obtain the title compound (8.11 g, 41.97 mmol, 71.97%) as a colorless oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07253286B2 |
| 出典データセット | uspto-grants-2007_08 |
| ORD ID | ord-51ba7a6db04e4598b99e8c14f289b527 |
| 出典メモ | uspto-grants-2007_08 |