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3-(Trifluoromethyl)benzaldehyde → 2-(3-Trifluoromethylphenyl)4-iodomethyl-5-methyloxazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-(Trifluoromethyl)benzaldehyde | HCID 67990 | — |
| 反応物 | 2,3-Butanedione monoxime | HCID 6409633 | — |
| 反応物 | 4-Iodomethyl-5-phenyl-2-p-tolyloxazole | HCID 57434504 | — |
| 生成物 | 2-(3-Trifluoromethylphenyl)4-iodomethyl-5-methyloxazole | HCID 22493681 | — |
反応手順
Analogously to the building block synthesis of 4-iodomethyl-5-phenyl-2-p-tolyloxazole, diacetylmonoxime and 3-trifluoromethylbenzaldehyde gave 4-iodomethyl-5-methyl-2-(3-trifluoromethylphenyl)oxazole.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07259177B2 |
| 出典データセット | uspto-grants-2007_08 |
| ORD ID | ord-33682384b87843048a23f598c9061b4a |
| 出典メモ | uspto-grants-2007_08 |