化工社化工社 化学情報印刷レポート · 研究参考用
Mannitol → Fentanyl
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Mannitol | HCID 6251 | — |
| 反応物 | Fentanyl Citrate | HCID 13810 | — |
| 反応物 | Aspartame | HCID 134601 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Fentanyl | HCID 3345 | — |
反応手順
Gelatin (765 g) and mannitol (540 g) were dispersed in a portion of purified water (16 kg) by mixing thoroughly in the bowl of a vacuum mixer. The mix was then heated to 40° C.±2° C. and homogenised for ten minutes to allow complete dissolution of the solids. The mix was cooled down to room temperature (20–24° C.). When cooled, the fentanyl citrate (22.68 g), the aspartame (90 g), and mint flavour (90 g) were added sequentially to the mix. The mix was then homogenized to ensure complete dissolution of the solids. The remaining water (492 g) was added to the mixer and the bulk mix homogenized to ensure dissolution was complete.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07090866B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-7699baaddd76414b851d402dc61a2e83 |
| 出典メモ | uspto-grants-2006_08 |